HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 19047231, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Butyryl chloride | HCID 8855 | — |
| Reactant | 12-Hydroxydodecanoic Acid | HCID 79034 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 19047231 | HCID 19047231 | 96.7% |
Reaction Steps
12-Hydroxydodecanoic acid (1 g) was dissolved in pyridine, and butyroyl chloride (0.59 g) was added to the solution in an ice bath. After 4 hours of stirring, the reaction mixture was distributed into chloroform and water , and the chloroform layer was concentrated to give 12-butyryloxydodecanoic acid (1.28 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05461036 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-9fa662eb78694448b64ae932189d1ff2 |
| Source note | uspto-grants-1995_10 |