1-Bromododecane → HCID 88419177, compound

HRID 2210886Notes

Reaction equation

HRID 2210886 reaction equation
C([N:13]1N=NC(CC(O)=O)=N1)CCCCCCCCCCC.S([O-])(=O)(=O)C.C[CH:28]([OH:39])CCCCCCCCCC.Br[CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH2:47][CH2:48][CH2:49][CH2:50][CH2:51][CH3:52].[CH:53]([C:56]1[CH:61]=[CH:60][CH:59]=[C:58]([CH:62]([CH3:64])[CH3:63])[C:57]=1[NH:65][C:66](=[O:86])[CH:67]([C:69]1[N:70]=[N:71][N:72](CCCCCCCCCCCC)[N:73]=1)Br)([CH3:55])[CH3:54]>>[CH:53]([C:56]1[CH:61]=[CH:60][CH:59]=[C:58]([CH:62]([CH3:64])[CH3:63])[C:57]=1[NH:65][C:66](=[O:86])/[C:67](/[C:69]1[N:70]=[N:71][N:72]([CH:51]([CH3:52])[CH2:50][CH2:49][CH2:48][CH2:47][CH2:46][CH2:45][CH2:44][CH2:43][CH2:42][CH3:41])[N:73]=1)=[N:13]/[O:39][CH3:28])([CH3:55])[CH3:54]

Participants

6

Reactant 5

HCID 89191-BromododecaneHCID 25045Dodecan-2-olHCID 85257MethanesulfonateHCID 10661649HCID 10661649, compoundHCID 15296921HCID 15296921, compound

Product 1

HCID 88419177HCID 88419177, compound

Procedure

When in the procedure of Example 13 (c) an appropriate amount of the mesylate of 2-dodecanol was substituted for 1-bromododecane and the general procedures for Example 13 (c), (d), and (e) were followed, E-N-(2,6-diisopropylphenyl)-2-(2-(1-methylundecyl) -2H-tetrazol-5-yl)-2-methoxyimino-acetamide was obtained;

Sources & evidence

ORD record
ord-9d26556df7f14e5b90f5737dbcb6e903
Source dataset
uspto-grants-1995_10
Patent number
US05461049

Reaction notes

Loading…