HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 131719154, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 131719155 | HCID 131719155 | — |
| Solvent | Ethanethiol | HCID 6343 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 131719154 | HCID 131719154 | — |
Reaction Steps
2.2 g (2.9 mmol) of H-Tyr(tBu)-Cys(Trt)-Asn-OtBu are dissolved in a mixture of 25 ml of trifluoroacetic acid and 25 ml of ethyl mercaptan. After 4 hours, the mixture is tipped into 250 ml of water. The aqueous solution is extracted 3 times with ether and freeze-dried. Yield 1.05 g (91%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05461035 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-724f40f40e0c4352bdfceb08eba58acd |
| Source note | uspto-grants-1995_10 |