2-(3-methylphenyl)thiophene → HCID 66608084, compound

HRID 221099Notes

Reaction equation

HRID 221099 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]([C:8]2[S:9][CH:10]=[CH:11][CH:12]=2)[CH:5]=[CH:6][CH:7]=1.[Br:13][C:14]1[CH:15]=[CH:16][C:17]([Cl:22])=[C:18]([CH:21]=1)[CH:19]=O>>[Br:13][C:14]1[CH:15]=[CH:16][C:17]([Cl:22])=[C:18]([CH2:19][C:10]2[S:9][C:8]([C:4]3[CH:5]=[CH:6][CH:7]=[C:2]([CH3:1])[CH:3]=3)=[CH:12][CH:11]=2)[CH:21]=1

Participants

3

Reactant 2

HCID 35641882-(3-methylphenyl)thiopheneHCID 106089255-Bromo-2-chlorobenzaldehyde

Product 1

HCID 66608084HCID 66608084, compound

Procedure

2-(3-Methylphenyl)thiophene obtained in Reference Example 83-(1) and 5-bromo-2-chlorobenzaldehyde obtained in Reference Example 16-(1) were treated in a manner similar to Reference Example 9 to give the target compound. APCI-Mass m/Z 377/379/381 (M+H).

Workup

  1. additionwere treated in a manner similar to Reference Example 9
  2. customto give the target compound

Sources & evidence

ORD record
ord-0a008f3dd7dd4086855d54394da1208d
Source dataset
uspto-grants-2012_06
Patent number
US08202984B2

Reaction notes

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