HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1-chloro-3-isocyanato- → 1-(3-Chlorophenylcarbamoyl)-2-nitroiminoimidazolidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1-chloro-3-isocyanato- | HCID 17968 | — |
| Reactant | N-nitroimidazolidin-2-imine | HCID 135413413 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 1-(3-Chlorophenylcarbamoyl)-2-nitroiminoimidazolidine | HCID 136342791 | — |
Reaction Steps
A solution of 3.9 g of 2-nitroiminoimidazolidine and 4.6 g of 3-chlorophenylisocyanate in 80 ml of dry acetonitrile was refluxed for 3 hours. After cooling to room temperature, the precipitated crystals were filtered, and washed with ether to give desired 1-(3-chlorophenylcarbamoyl)-2-nitroiminoimidazolidine. The yield was 4.7 g. mp. 214°-216° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05461167 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-bcc1de2de5ce425baad7b7a3adfc94b8 |
| Source note | uspto-grants-1995_10 |