HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Toluenesulfonyl chloride → HCID 54574482, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 53666096 | HCID 53666096 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54574482 | HCID 54574482 | — |
Reaction Steps
21 g of 2-aminoindan-5-yl-3-pyridyl ketone are dissolved together with 18.9 g of p-toluenesulphonic acid chloride in 250 ml of methylene chloride. Then 9.2 g of triethylamine are added dropwise. After 4 hours the suspension is rotary-evaporated to dryness. The residue is suspended in water, made alkaline with sodium hydroxide solution and then suction filtered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05426119 |
| Source dataset | uspto-grants-1995_06 |
| ORD ID | ord-fc2441b21c7848fe9e836638258d0816 |
| Source note | uspto-grants-1995_06 |