HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 19375607, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 2-(Thiophene-3-carbonyl)benzoic acid | HCID 13554735 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19375607 | HCID 19375607 | 51.4% |
Reaction Steps
1.8 g of o-(3-thenoyl)benzoic acid and 580 mg of hydrazine hydrate were dissolved in 20 ml of ethanol, and the solution was refluxed for 4 hours. After cooling the solution, it was crystallized by adding ether, thereby obtaining 910 mg of 4-(3-thienyl)-1-phthalazinone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05462941 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-0c5e4e9cb4ef48c4967f66babd00c4b7 |
| Source note | uspto-grants-1995_10 |