HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 19376852, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Allyl Mercaptan | HCID 13367 | — |
| Product | HCID 19376852 | HCID 19376852 | — |
Reaction Steps
A solution of 2-(3-oxetane)butyl tosylate of example 3 in an inert solvent such as THF is stirred with one equivalent of allyl mercaptan at room temperature until reaction is complete. The solvent is stripped and the residue taken up in ether. The ether is washed with saturated aqueous NaHCO3, dried over MgSO4 and stripped to provide 3-ethyl-3-allythiomethyloxetane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05463084 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-d71ea15015d8459183c9318c5bbacf7c |
| Source note | uspto-grants-1995_10 |