Cyanamide → HCID 178499797, compound

HRID 2211280Notes

Reaction equation

HRID 2211280 reaction equation
[ClH:1].[NH2:2][C:3]1[CH:4]=[C:5]([C:9]2[N:10]=[C:11]([C:14]3[CH:19]=[CH:18][C:17]([CH2:20][CH2:21][C:22]([O:24][CH3:25])=[O:23])=[CH:16][CH:15]=3)[NH:12][CH:13]=2)[CH:6]=[CH:7][CH:8]=1.[N:26]#[C:27][NH2:28]>O1CCOCC1>[ClH:1].[NH:2]([C:3]1[CH:4]=[C:5]([C:9]2[N:10]=[C:11]([C:14]3[CH:19]=[CH:18][C:17]([CH2:20][CH2:21][C:22]([O:24][CH3:25])=[O:23])=[CH:16][CH:15]=3)[NH:12][CH:13]=2)[CH:6]=[CH:7][CH:8]=1)[C:27]([NH2:28])=[NH:26]

Participants

4

Reactant 2

HCID 9864CyanamideHCID 178499796HCID 178499796, compound

Product 1

HCID 178499797HCID 178499797, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

Prepared from 4-(3-amino-phenyl)-2-[4-(2-methoxycarbonyl-ethyl)-phenyl]-imidazole-hydrochloride by refluxing for three hours with cyanamide in dioxane.

Sources & evidence

ORD record
ord-981250ac03df43dcb61b8886956e137a
Source dataset
uspto-grants-1995_10
Patent number
US05463071

Reaction notes

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