HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfolane → 1,1,1,4,4,4-Hexafluoro-2-butene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfolane | HCID 31347 | — |
| Reactant | Potassium Fluoride | HCID 522689 | — |
| Reactant | 2-Chloro-1,1,1,4,4,4-hexafluorobutane | HCID 2736596 | — |
| Product | 1,1,1,4,4,4-Hexafluoro-2-butene | HCID 2774975 | — |
Reaction Steps
200 g of 2-chloro-1,1,1,4,4,4-hexafluorobutane were added dropwise to a mixture of 195 ml of distilled tetramethylene sulphone and 87 g of dried potassium fluoride at 190° C. and the 1,1,1,4,4,4-hexafluorobut-2-ene which formed was continuously distilled off. 135 g of 1,1,1,4,4,4-hexafluorobut-2-ene were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05463150 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-80b3e330653f443b932f2746d73a47fa |
| Source note | uspto-grants-1995_10 |