2-Phenylthiophene → HCID 66607795, compound

HRID 221140Notes

Reaction equation

HRID 221140 reaction equation
[Br:1][C:2]1[S:6][C:5]([Cl:7])=[C:4]([C:8](O)=O)[CH:3]=1.[C:11]1([C:17]2[S:18][CH:19]=[CH:20][CH:21]=2)[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1>>[Br:1][C:2]1[S:6][C:5]([Cl:7])=[C:4]([CH2:8][C:19]2[S:18][C:17]([C:11]3[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=3)=[CH:21][CH:20]=2)[CH:3]=1

Participants

3

Reactant 2

HCID 699992-PhenylthiopheneHCID 22397190HCID 22397190, compound

Product 1

HCID 66607795HCID 66607795, compound

Procedure

5-Bromo-2-chloro-3-thiophenecarboxylic acid (see Japanese Unexamined Patent Publication No. 10-324632) and 2-phenylthiophene were treated in a manner similar to Reference Example 5 to give the target compound as a colorless solid. APCI-Mass m/Z 367/369 (M+H).

Sources & evidence

ORD record
ord-b687f66632564aa981d37c4ac8d58805
Source dataset
uspto-grants-2012_06
Patent number
US08202984B2

Reaction notes

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