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Potassium Carbonate → 4-[2-[2-Methyl-4-oxo-3,4-dihydro-3-quinazolinyl]ethoxy]benzaldehyde
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | 4-(2-Bromoethoxy)Benzaldehyde | HCID 262706 | — |
| 反応物 | 2-Methyl-4(3H)-quinazolinone | HCID 135400457 | — |
| 生成物 | 4-[2-[2-Methyl-4-oxo-3,4-dihydro-3-quinazolinyl]ethoxy]benzaldehyde | HCID 21960134 | 39% |
反応手順
The title compound (0.6 g, 39%) was prepared from 2-methyl-4-oxo-3,4-dihydroquinazoline (0.8 g, 5 mmol) and 4-[2-bromoethoxy]benzaldehyde (1.37 g, 6 mmol) in the presence of K2CO3 (1.38 g, 10.0 mmol) as base, by a similar procedure to that described is preparation 1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | USRE039266E1 |
| 出典データセット | uspto-grants-2006_09 |
| ORD ID | ord-f6ad941d19cc4e868a5b487eb1675f8f |
| 出典メモ | uspto-grants-2006_09 |