HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(4-hydroxy-2,3,6-trimethylphenyl)formamide → HCID 73856747, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(4-hydroxy-2,3,6-trimethylphenyl)formamide | HCID 21961295 | — |
| Reactant | HCID 54503384 | HCID 54503384 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 73856747 | HCID 73856747 | 41% |
Reaction Steps
By using N-(4-hydroxy-2,3,6-trimethylphenyl)formamide and 1-(3-bromo-2-methyl-1-propenyl)benzene, the title compound was synthesized according to Reference Example 17b. Yield: 41%. Melting point: 152-154° C. (Ethyl acetate-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07101867B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-7b8e74813c6045d19f52812ccfcddd25 |
| Source note | uspto-grants-2006_09 |