HuagongsheHuagongshe Chemistry Print Report · For research reference only
53041-12-6 → HCID 21961349, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 53041-12-6 | HCID 11830831 | — |
| Reactant | N-(4-hydroxy-2,3,6-trimethylphenyl)formamide | HCID 21961295 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 21961349 | HCID 21961349 | 52% |
Reaction Steps
By using N-(4-hydroxy-2,3,6-trimethylphenyl)formamide and 1-[(E)-3-bromo-1-propenyl]-4-fluorobenzene, the title compound was synthesized according to Reference Example 17b. Yield: 52%. Melting point: 196-198° C. (Ethyl acetate-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07101867B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-b90f8652123a4364beca0668bf17f36b |
| Source note | uspto-grants-2006_09 |