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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2211770Generated: November 1, 2026

1,3-Benzodioxole-5-carbonyl chloride → HCID 10183771, compound

https://huagongshe.com/reaction/2211770

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,3-Benzodioxole-5-carbonyl chlorideHCID 2734749—
Reactant3-(4-Isopropylphenyl)-2,2,4,6,7-pentamethyl-2,3-dihydro-1-benzofuran-5-amineHCID 10519978—
SolventDiethylether hexaneHCID 21584099—
ProductHCID 10183771HCID 1018377167%

Reaction Steps

By using 3-(4-isopropylphenyl)-2,2,4,6,7-pentamethyl-2,3-dihydro-1-benzofuran-5-amine and 1,3-benzodioxol-5-carbonyl chloride, the title compound was synthesized according to Example 1b. Yield: 67%. Melting point: 165-167° C. (Ethyl ether-hexane).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07101867B2
Source datasetuspto-grants-2006_09
ORD IDord-4dc5a3bc18884439a6d02067158b2027
Source noteuspto-grants-2006_09