HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl chloromethyl ether → tert-Butyl 4-[(benzyloxy)methyl]hexahydro-2-methylene-3-oxo-1,4-diazepine-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl chloromethyl ether | HCID 137983 | — |
| Reactant | tert-Butyl 4-[(Benzyloxy)methyl]hexahydro-3-oxo-1H-1,4-diazepine-1-carboxylate | HCID 21962085 | — |
| Product | tert-Butyl 4-[(benzyloxy)methyl]hexahydro-2-methylene-3-oxo-1,4-diazepine-1-carboxylate | HCID 21962090 | — |
Reaction Steps
The title was prepared from tert-butyl 4-[(benzyloxy)methyl]hexahydro-3-oxo-1H-1,4-diazepine-1-carboxylate and benzyl chloromethyl ether essentially following the procedure described in Example 3, Step 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07101871B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-c4d802a4e54a4056b84e1ba1c27b7cf7 |
| Source note | uspto-grants-2006_09 |