HCID 131728098, compound → 2-Sulfanylundecanoic acid

HRID 221185Notes

Reaction equation

HRID 221185 reaction equation
[SH:1][CH:2]([CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14])[C:3]([OH:5])=[O:4].CO>[Se-2].[Cd+2]>[SH:1][CH:2]([CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14])[C:3]([OH:5])=[O:4]

Participants

3

Reactant 1

HCID 131728098HCID 131728098, compound

Product 1

HCID 219323062-Sulfanylundecanoic acid

Reagents, catalysts & solvents 1

HCID 98370071306-24-7Solvent

Procedure

In the absence of light, the precipitated CdSe nanocrystals are dissolved in the MUA-methanol solution. The resulting solution is stirred under an Argon flow for about 2 hours to form mercaptoundecanoic acid (MUA)-capped CdSe nanocrystals. Ethyl acetate and ethyl ether are used to precipitate and wash (repeatedly between about 2 and 3 times) the MUA-capped CdSe nanocrystals. Subsequently, the MUA-capped CdSe nanocrystals preferably are dispersed in isopropanol to define a cadmium selenide (CdSe) solution.

Sources & evidence

ORD record
ord-b80ea75d1a654cc59ecbbeb9f1e5f6b8
Source dataset
uspto-grants-2012_06
Patent number
US08206824B2

Reaction notes

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