HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Pyrocarbonate → HCID 21964591, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Pyrocarbonate | HCID 3051 | — |
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | HCID 69584976 | HCID 69584976 | — |
| Product | HCID 21964591 | HCID 21964591 | — |
Reaction Steps
Following the procedure for preparation of 106, and substituting ethyl chloroformate and 108 with diethyl pyrocarbonate and 102, respectively, provided the title compound. 1H NMR (CD3OD, 400 MHz): 1.18 (t, 6H), 1.36 (s, 3H), 3.01 (dd, 2H), 3.80 (s, 3H), 4.17 (q, 4H), 7.08–7.17 (m, 3H). MS (ESI) m/z 371.24 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07101912B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-d70d74a7253d4260a5aab504b8fe8835 |
| Source note | uspto-grants-2006_09 |