HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenoxyethanol → 3-(3,4-Dihydroxy-phenyl)-2-hydrazino-2-methyl-propionic Acid 2-phenoxy-ethyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenoxyethanol | HCID 31236 | — |
| Reactant | Methyl 3-(3,4-dihydroxyphenyl)-2-hydrazinyl-2-methylpropanoate | HCID 13589972 | — |
| Product | 3-(3,4-Dihydroxy-phenyl)-2-hydrazino-2-methyl-propionic Acid 2-phenoxy-ethyl Ester | HCID 69584974 | — |
Reaction Steps
Following the procedure described in Example 4 Step A for preparation of compound 107, and substituting methanol with 2-phenoxy-ethanol, provided the title compound. 1H NMR (CD3OD, 400 MHz): 1.65 (s, 3H), 3.10 (dd, 2H), 4.40 (t, 2H), 4.70 (t, 2H), 6.60–6.52 (m, 8H). MS (ESI) m/z 347.27 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07101912B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-aa31ddc82ca545bfb5adca1296790199 |
| Source note | uspto-grants-2006_09 |