HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pivaloyl chloride → HCID 69584924, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pivaloyl chloride | HCID 62493 | — |
| Reactant | HCID 69585130 | HCID 69585130 | — |
| Product | HCID 69584924 | HCID 69584924 | — |
Reaction Steps
Following the procedure for preparation of compound 101, and substituting ethyl chloroformate with 2,2-dimethylpropionyl chloride, provided the title compound. 1H NMR (CD3OD, 400 MHz): δ 1.33 (s, 9H), 1.34 (s, 9H), 1.46 (s, 3H), 2.12 (s, 3H), 3.08 (dd, 2H), 5.83 (dd, 2H), 7.05–7.12 (m, 3H). MS (ESI) m/z 467.35 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07101912B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-5d2c5cc96db748638a2d1f2249dbb1a4 |
| Source note | uspto-grants-2006_09 |