Methanol → HCID 59896206, compound

HRID 2212620Notes

Reaction equation

HRID 2212620 reaction equation
[NH2:1][CH2:2][CH2:3][S:4][CH2:5][C@@H:6]([C:8]([OH:10])=[O:9])[NH2:7].[CH3:11]O>>[NH2:1][CH2:2][CH2:3][S:4][CH2:5][C@@H:6]([C:8]([O:10][CH3:11])=[O:9])[NH2:7]

Participants

3

Reactant 2

HCID 887MethanolHCID 99558S-(2-Aminoethyl)-L-cysteine

Product 1

HCID 59896206HCID 59896206, compound

Procedure

A 10 g (50 mmol) sample of S-(2-aminoethyl)-L-cysteine was dissolved in 400 mL of methanol. Into this cooled solution was bubbled in anhydrous HCl for 30 minutes. After stirring at room temperature overnight, the solution was concentrated to afford 12.7 g of the title compound.

Workup

  1. customInto this cooled solution was bubbled in anhydrous HCl for 30 minutes
  2. concentrationthe solution was concentrated

Sources & evidence

ORD record
ord-6d845bb2135b4f2eb5c19437b15f5d94
Source dataset
uspto-grants-2006_09
Patent number
US07102013B2

Reaction notes

Loading…