Sodium Hydroxide → L-Leucine

HRID 2212792Notes

Reaction equation

HRID 2212792 reaction equation
Cl.[NH2:2][C@H:3]([C:8]([OH:10])=[O:9])[CH2:4][CH:5]([CH3:7])[CH3:6].[OH-].[Na+]>O>[NH2:2][C@H:3]([C:8]([OH:10])=[O:9])[CH2:4][CH:5]([CH3:7])[CH3:6]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 102479Leucine hydrochloride

Product 1

HCID 6106L-Leucine

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A similar dispersion was prepared with the use of Pluronic F-68 as stabilizer. An amount of 0.152 grams of leucine hydrochloride was added to 0.852 grams of nanostructured reverse bicontinuous cubic phase material as above, and an upper phase consisting of 0.08 grams of F-68, 1.0 gram of 1 M sodium hydroxide, and 3.0 grams of water was overlaid on the nanostructured reverse bicontinuous cubic phase material and sonicated. Again, a milky-white dispersion of leucine-coated microparticles was formed, where this time the F-68 amphiphilic block copolymer surfactant coated the outer (leucine-based) surface of the particles.

Workup

  1. customsonicated

Sources & evidence

ORD record
ord-7140d95392874d15b7b2d33edffededd
Source dataset
uspto-grants-2006_09
Patent number
US07105229B2

Reaction notes

Loading…