HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → 1-Cyclohexyl-4-[2-(ethenyloxy)ethoxy]benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 4-Ethynylphenol | HCID 32758 | — |
| Product | 1-Cyclohexyl-4-[2-(ethenyloxy)ethoxy]benzene | HCID 22011687 | — |
Reaction Steps
In 80 ml of THF were dissolved 20 g of poly(p-hydroxystyrene), VP-8000 (produced by Nippon Soda Co., Ltd.), and 6.5 g of 4-cyclohexylphenoxyethyl vinyl ether. Thereto, 0.01 g of p-toluenesulfonic acid was added. The resulting mixture underwent reaction for 18 hours at room temperature. The reaction solution was dripped into 5L of distilled water with vigorous stirring, and fine solid particles precipitated out were filtered off and dried. Thus, Polymer (B-32) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07105273B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-5fb8cbbf391e44119b717142de225f37 |
| Source note | uspto-grants-2006_09 |