HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23518325, compound → HCID 23518327, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23518325 | HCID 23518325 | — |
| Solvent | Ammonia | HCID 222 | — |
| Product | HCID 23518327 | HCID 23518327 | 100.6% |
Reaction Steps
A mixture of the compound from Step F (0.27 g, 0.53 mmol) and methanolic ammonia (saturated at 0° C.; 10 mL) was kept overnight at 0° C. Evaporation of the solvent yielded the desired compound (0.25 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07105499B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-5612855732c34a9981add76caf9745bc |
| Source note | uspto-grants-2006_09 |