HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfamethizole → HCID 178434114, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfamethizole | HCID 5328 | — |
| Reactant | 8-[Ethoxymethylidene]-6H-[1,3]thiazolo[5,4-e]indol-7-one | HCID 53990807 | — |
| Product | HCID 178434114 | HCID 178434114 | 36% |
Reaction Steps
The title compound was prepared in 36% yield from 8-ethoxymethylene-6,8-dihydro-1-thia-3,6-diaza-as-indacen-7-one and 4-amino-N-(5-methyl[1,3,4]thiadiazol-2-yl)-benzenesulfonamide according to Procedure J: 1H NMR (DMSO-d6): δ 11.2 (d, 1H), 10.9 (s, 1H), 9.3 (s, 1H), 8.1 (d, 1H), 7.8 (m, 3H), 7.6 (d, 2H), 7.1 (d, 1H); ESI-MS m/z 469 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07105529B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-cd6fc9e6964a429ea864fb82d03b3d8d |
| Source note | uspto-grants-2006_09 |