HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-Indazol-6-amine → HCID 21956186, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-Indazol-6-amine | HCID 81423 | — |
| Reactant | 3-(hydroxymethylidene)-1H-indol-2-one | HCID 178418741 | — |
| Product | HCID 21956186 | HCID 21956186 | 79% |
Reaction Steps
The title compound was prepared in 79% yield from 3-hydroxymethylene-1,3-dihydro-indol-2-one and 6-aminoindazole according to Procedure J: 1H NMR (DMSO-d6): δ 13.02 (s, 1H), 10.86 (d, 1H), 10.51 (s, 1H), 8.7 (d, 1H), 8.0 (s, 1H), 7.74 (d, 1H), 7.63 (d, 1H), 7.51 (s, 1H), 7.15 (dd, 1H), 7.02 (m, 1H), 6.94 (m, 1H), 6.85 (d, 1H); ESI-MS m/z 275 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07105529B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-f51b4cb1a2de47af9f948bfab96305bf |
| Source note | uspto-grants-2006_09 |