HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Chlorophenyl)cyclopentanecarboxylic acid → HCID 21957232, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Chlorophenyl)cyclopentanecarboxylic acid | HCID 97447 | — |
| Reactant | N-{3-[1-(3-aminopropyl)4-piperidinyl]phenyl}cyclopropanecarboxamide | HCID 21957166 | — |
| Product | HCID 21957232 | HCID 21957232 | — |
Reaction Steps
Example 112 was prepared from 1-(4-chlorophenyl)cyclopentanecarboxylic acid and N-{3-[1-(3-aminopropyl)-4-piperidinyl]phenyl}cyclopropanecarboxamide according to the procedures described in Scheme 10: 1H NMR (400 MHz, CDCl3) δ 8.03–7.87 (br, 1H), 7.56–7.02 (m, 8H), 6.91–6.65 (br, 1H), 3.30–3.05 (m, 4H), 2.62–2.38 (m, 3H), 2.38–2.21 (m, 2H), 1.98–1.51 (m, 15H), 1.14–1.01 (m, 2H), 0.93–0.70 (m, 2H) ESMS m/e: 508.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07105544B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-af4e9d2c87b141ba8fa2e9e86bef02e6 |
| Source note | uspto-grants-2006_09 |