4-(Dimethylamino)Benzaldehyde → (4-Butylphenyl)[(4-dimethylaminophenyl)methyl]amine

HRID 2213583Notes

Reaction equation

HRID 2213583 reaction equation
[CH3:1][N:2]([CH3:11])[C:3]1[CH:10]=[CH:9][C:6]([CH:7]=O)=[CH:5][CH:4]=1.[CH2:12]([C:16]1[CH:22]=[CH:21][C:19]([NH2:20])=[CH:18][CH:17]=1)[CH2:13][CH2:14][CH3:15]>>[CH2:12]([C:16]1[CH:17]=[CH:18][C:19]([NH:20][CH2:7][C:6]2[CH:9]=[CH:10][C:3]([N:2]([CH3:11])[CH3:1])=[CH:4][CH:5]=2)=[CH:21][CH:22]=1)[CH2:13][CH2:14][CH3:15]

Participants

3

Reactant 2

HCID 74794-(Dimethylamino)BenzaldehydeHCID 76944-Butylaniline

Product 1

HCID 21957943(4-Butylphenyl)[(4-dimethylaminophenyl)methyl]amineYield 36.1%

Procedure

By the reaction and treatment in the same manner as in Preparation Example 1 using 4-dimethylaminobenzaldehyde (10.0 g) and 4-butylaniline (10.0 g) as starting materials, (4-butylphenyl)[(4-dimethylaminophenyl)methyl]amine (6.83 g) was obtained. melting point: 60–61° C.

Workup

  1. customBy the reaction and treatment in the same manner

Sources & evidence

ORD record
ord-20df0cbc23c54e46a56e537a7fdc4b44
Source dataset
uspto-grants-2006_09
Patent number
US07105567B2

Reaction notes

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