4-(Dimethylamino)Benzaldehyde → [(4-Dimethylaminophenyl)methyl](4-propylphenyl)amine

HRID 2213586Notes

Reaction equation

HRID 2213586 reaction equation
[CH3:1][N:2]([CH3:11])[C:3]1[CH:10]=[CH:9][C:6]([CH:7]=O)=[CH:5][CH:4]=1.[CH2:12]([C:15]1[CH:21]=[CH:20][C:18]([NH2:19])=[CH:17][CH:16]=1)[CH2:13][CH3:14]>>[CH3:1][N:2]([CH3:11])[C:3]1[CH:10]=[CH:9][C:6]([CH2:7][NH:19][C:18]2[CH:20]=[CH:21][C:15]([CH2:12][CH2:13][CH3:14])=[CH:16][CH:17]=2)=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 74794-(Dimethylamino)BenzaldehydeHCID 759084-Propylaniline

Product 1

HCID 21957946[(4-Dimethylaminophenyl)methyl](4-propylphenyl)amineYield 88.9%

Procedure

By the reaction and treatment in the same manner as in Preparation Example 1 using 4-dimethylaminobenzaldehyde (11 g) and 4-propylaniline (10 g) as starting materials, [(4-dimethylaminophenyl)methyl](4-propylphenyl)amine (17.6 g) was obtained. melting point: 74–76° C.

Workup

  1. customBy the reaction and treatment in the same manner

Sources & evidence

ORD record
ord-ec6491252ae0416a9b7096bcc365fb10
Source dataset
uspto-grants-2006_09
Patent number
US07105567B2

Reaction notes

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