4-(Dimethylamino)Benzaldehyde → HCID 5183485, compound

HRID 2213588Notes

Reaction equation

HRID 2213588 reaction equation
[CH3:1][N:2]([CH3:11])[C:3]1[CH:10]=[CH:9][C:6]([CH:7]=O)=[CH:5][CH:4]=1.[CH2:12]([O:14][C:15]1[CH:21]=[CH:20][C:18]([NH2:19])=[CH:17][CH:16]=1)[CH3:13]>>[CH3:1][N:2]([CH3:11])[C:3]1[CH:10]=[CH:9][C:6]([CH2:7][NH:19][C:18]2[CH:20]=[CH:21][C:15]([O:14][CH2:12][CH3:13])=[CH:16][CH:17]=2)=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 74794-(Dimethylamino)BenzaldehydeHCID 90764-Ethoxyaniline

Product 1

HCID 5183485HCID 5183485, compoundYield 44.1%

Procedure

By the reaction and treatment in the same manner as in Preparation Example 1 using 4-dimethylaminobenzaldehyde (11 g) and 4-ethoxyaniline (10 g) as starting materials, [(4-dimethylaminophenyl)methyl](4-ethoxyphenyl)amine (8.7 g) was obtained. melting point: 98–99° C.

Workup

  1. customBy the reaction and treatment in the same manner

Sources & evidence

ORD record
ord-c5b1c7fee3b143d4b6a93b2b2943f125
Source dataset
uspto-grants-2006_09
Patent number
US07105567B2

Reaction notes

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