3,4-Dimethylaniline → HCID 3544717, compound

HRID 2213590Notes

Reaction equation

HRID 2213590 reaction equation
[CH3:1][N:2]([CH3:11])[C:3]1[CH:10]=[CH:9][C:6]([CH:7]=O)=[CH:5][CH:4]=1.[CH3:12][C:13]1[CH:14]=[C:15]([CH:17]=[CH:18][C:19]=1[CH3:20])[NH2:16]>>[CH3:1][N:2]([CH3:11])[C:3]1[CH:10]=[CH:9][C:6]([CH2:7][NH:16][C:15]2[CH:17]=[CH:18][C:19]([CH3:20])=[C:13]([CH3:12])[CH:14]=2)=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 72483,4-DimethylanilineHCID 74794-(Dimethylamino)Benzaldehyde

Product 1

HCID 3544717HCID 3544717, compoundYield 55.6%

Procedure

By the reaction and treatment in the same manner as in Preparation Example 1 using 4-dimethylaminobenzaldehyde (1.5 g) and 3,4-dimethylaniline (1.2 g) as starting materials, [(4-dimethylaminophenyl)methyl](3,4-dimethylphenyl)amine (1.4 g) was obtained. melting point: 73–75° C.

Workup

  1. customBy the reaction and treatment in the same manner

Sources & evidence

ORD record
ord-1c6a30ea8d854a64911b66d70cd3d588
Source dataset
uspto-grants-2006_09
Patent number
US07105567B2

Reaction notes

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