2,4-Dimethylaniline → HCID 3709822, compound

HRID 2213593Notes

Reaction equation

HRID 2213593 reaction equation
[CH3:1][N:2]([CH3:11])[C:3]1[CH:10]=[CH:9][C:6]([CH:7]=O)=[CH:5][CH:4]=1.[CH3:12][C:13]1[CH:19]=[C:18]([CH3:20])[CH:17]=[CH:16][C:14]=1[NH2:15]>>[CH3:1][N:2]([CH3:11])[C:3]1[CH:10]=[CH:9][C:6]([CH2:7][NH:15][C:14]2[CH:16]=[CH:17][C:18]([CH3:20])=[CH:19][C:13]=2[CH3:12])=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 72502,4-DimethylanilineHCID 74794-(Dimethylamino)Benzaldehyde

Product 1

HCID 3709822HCID 3709822, compoundYield 95.3%

Procedure

By the reaction and treatment in the same manner as in Preparation Example 1 using 4-dimethylaminobenzaldehyde (1.5 g) and 2,4-dimethylaniline (1.2 g) as starting materials, [(4-dimethylaminophenyl)methyl](2,4-dimethylphenyl)amine (2.4 g) was obtained. melting point: 79–80° C.

Workup

  1. customBy the reaction and treatment in the same manner

Sources & evidence

ORD record
ord-2f72d19269b1473da3c242b80cb13a37
Source dataset
uspto-grants-2006_09
Patent number
US07105567B2

Reaction notes

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