3,4-Dichloroaniline → HCID 5183484, compound

HRID 2213599Notes

Reaction equation

HRID 2213599 reaction equation
[CH3:1][N:2]([CH3:11])[C:3]1[CH:10]=[CH:9][C:6]([CH:7]=O)=[CH:5][CH:4]=1.[Cl:12][C:13]1[CH:14]=[C:15]([CH:17]=[CH:18][C:19]=1[Cl:20])[NH2:16]>>[Cl:12][C:13]1[CH:14]=[C:15]([NH:16][CH2:7][C:6]2[CH:9]=[CH:10][C:3]([N:2]([CH3:11])[CH3:1])=[CH:4][CH:5]=2)[CH:17]=[CH:18][C:19]=1[Cl:20]

Participants

3

Reactant 2

HCID 72573,4-DichloroanilineHCID 74794-(Dimethylamino)Benzaldehyde

Product 1

HCID 5183484HCID 5183484, compoundYield 61.7%

Procedure

By the reaction and treatment in the same manner as in Preparation Example 1 using 4-dimethylaminobenzaldehyde (1.5 g) and 3,4-dichloroaniline (1.6 g) as starting materials, (3,4-dichlorophenyl)[(4-dimethylaminophenyl)methyl]amine (1.8 g) was obtained. melting point: 117° C.

Workup

  1. customBy the reaction and treatment in the same manner

Sources & evidence

ORD record
ord-e95a4db74ad5455c94c826eb86d3cfed
Source dataset
uspto-grants-2006_09
Patent number
US07105567B2

Reaction notes

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