2,6-Diisopropylphenyl isocyanate → HCID 12972747, compound

HRID 2213605Notes

Reaction equation

HRID 2213605 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([CH2:10][NH:11][C:12]2[CH:17]=[CH:16][C:15]([CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25])=[CH:14][CH:13]=2)=[CH:6][CH:5]=1)([O-:3])=[O:2].[CH:26]([C:29]1[CH:34]=[CH:33][CH:32]=[C:31]([CH:35]([CH3:37])[CH3:36])[C:30]=1[N:38]=[C:39]=[O:40])([CH3:28])[CH3:27]>>[CH:26]([C:29]1[CH:34]=[CH:33][CH:32]=[C:31]([CH:35]([CH3:36])[CH3:37])[C:30]=1[NH:38][C:39](=[O:40])[N:11]([CH2:10][C:7]1[CH:6]=[CH:5][C:4]([N+:1]([O-:3])=[O:2])=[CH:9][CH:8]=1)[C:12]1[CH:13]=[CH:14][C:15]([CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25])=[CH:16][CH:17]=1)([CH3:27])[CH3:28]

Participants

3

Reactant 2

HCID 922592,6-Diisopropylphenyl isocyanateHCID 21957921HCID 21957921, compound

Product 1

HCID 12972747HCID 12972747, compoundYield 6.5%

Procedure

By the reaction and treatment in the same manner as in Example 2 using [(4-nitrophenyl)methyl](4-octylphenyl)amine (2.6 g) and 2,6-diisopropylphenyl isocyanate (1.55 g) as starting materials, N′-(2,6-diisopropylphenyl)-N-[(4-nitrophenyl)methyl]-N-(4-octylphenyl)urea (0.27 g) was obtained.

Sources & evidence

ORD record
ord-bea9bec118ac4182926e97af89f2b2e1
Source dataset
uspto-grants-2006_09
Patent number
US07105567B2

Reaction notes

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