2,6-Diisopropylphenyl isocyanate → HCID 21957931, compound

HRID 2213613Notes

Reaction equation

[CH2:1]([C:9]1[CH:14]=[CH:13][C:12]([NH:15][CH2:16][C:17]2[CH:22]=[CH:21][C:20]([O:23][C:24]3[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=3)=[CH:19][CH:18]=2)=[CH:11][CH:10]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[CH:30]([C:33]1[CH:38]=[CH:37][CH:36]=[C:35]([CH:39]([CH3:41])[CH3:40])[C:34]=1[N:42]=[C:43]=[O:44])([CH3:32])[CH3:31]>>[CH:30]([C:33]1[CH:38]=[CH:37][CH:36]=[C:35]([CH:39]([CH3:40])[CH3:41])[C:34]=1[NH:42][C:43](=[O:44])[N:15]([C:12]1[CH:13]=[CH:14][C:9]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8])=[CH:10][CH:11]=1)[CH2:16][C:17]1[CH:18]=[CH:19][C:20]([O:23][C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=2)=[CH:21][CH:22]=1)([CH3:31])[CH3:32]

Participants

Reactant 2

HCID 922592,6-Diisopropylphenyl isocyanate

HCID 21957894HCID 21957894, compound

Product 1

HCID 21957931HCID 21957931, compoundYield 23.6%

Procedure

By the reaction and treatment in the same manner as in Example 2 using (4-octylphenyl)[(4-phenoxyphenyl)methyl]amine (1.53 g) and 2,6-diisopropylphenyl isocyanate (0.88 g) as starting materials, N′-(2,6-diisopropylphenyl)-N-(4-octylphenyl)-N-[(4-phenoxyphenyl)methyl]urea (0.55 g) was obtained.

Sources & evidence

ORD record: ord-5941286b2c8946dd9e6b683d011a3bb9
Source dataset: uspto-grants-2006_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07105567B2

Reaction notes

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