2,6-Diisopropylphenyl isocyanate → HCID 21957927, compound

HRID 2213618Notes

Reaction equation

[CH2:1]([C:9]1[CH:14]=[CH:13][C:12]([NH:15][CH2:16][C:17]2[CH:26]=[CH:25][C:20]([C:21]([O:23][CH3:24])=[O:22])=[CH:19][CH:18]=2)=[CH:11][CH:10]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[CH:27]([C:30]1[CH:35]=[CH:34][CH:33]=[C:32]([CH:36]([CH3:38])[CH3:37])[C:31]=1[N:39]=[C:40]=[O:41])([CH3:29])[CH3:28]>>[CH:27]([C:30]1[CH:35]=[CH:34][CH:33]=[C:32]([CH:36]([CH3:37])[CH3:38])[C:31]=1[NH:39][C:40](=[O:41])[N:15]([CH2:16][C:17]1[CH:26]=[CH:25][C:20]([C:21]([O:23][CH3:24])=[O:22])=[CH:19][CH:18]=1)[C:12]1[CH:13]=[CH:14][C:9]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8])=[CH:10][CH:11]=1)([CH3:28])[CH3:29]

Participants

Reactant 2

HCID 922592,6-Diisopropylphenyl isocyanate

HCID 21957900HCID 21957900, compound

Product 1

HCID 21957927HCID 21957927, compoundYield 6.9%

Procedure

By the reaction and treatment in the same manner as in Example 2 using methyl 4-[(4-octylphenyl)aminomethyl]benzoate (2.65 g) and 2,6-diisopropylphenyl isocyanate (1.68 g) as starting materials, methyl 4-{[3-(2,6-diisopropylphenyl)-1-(4-octylphenyl)ureido]methyl}benzoate (0.29 g) was obtained.

Sources & evidence

ORD record: ord-8a6f6b5b0e1d419eb811a027cefc5881
Source dataset: uspto-grants-2006_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07105567B2

Reaction notes

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