HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Diisopropylphenyl isocyanate → N-(4-bromophenyl)-N'-(2,6-diisopropylphenyl)-N-[(4-dimethylaminophenyl)methyl]urea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Diisopropylphenyl isocyanate | HCID 92259 | — |
| Reactant | 4-[(4-Bromoanilino)methyl]-N,N-dimethylaniline | HCID 15174101 | — |
| Product | N-(4-bromophenyl)-N'-(2,6-diisopropylphenyl)-N-[(4-dimethylaminophenyl)methyl]urea | HCID 21957958 | — |
Reaction Steps
By the reaction and treatment in the same manner as in Example 1 using (4-bromophenyl)[(4-dimethylaminophenyl)methyl]amine (0.80 g) and 2,6-diisopropylphenyl isocyanate (0.62 mL) as starting materials, N-(4-bromophenyl)-N′-(2,6-diisopropylphenyl)-N-[(4-dimethylaminophenyl)methyl]urea (0.71 g) was obtained. melting point: 165–166° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07105567B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-be01102d1769416289cfe98b20d8d26a |
| Source note | uspto-grants-2006_09 |