2,6-Diisopropylphenyl isocyanate → HCID 21957915, compound

HRID 2213639Notes

Reaction equation

HRID 2213639 reaction equation
[CH3:1][N:2]([CH3:21])[C:3](=[O:20])[C:4]1[CH:9]=[CH:8][C:7]([CH2:10][NH:11][C:12]2[CH:17]=[CH:16][C:15]([CH2:18][CH3:19])=[CH:14][CH:13]=2)=[CH:6][CH:5]=1.[CH:22]([C:25]1[CH:30]=[CH:29][CH:28]=[C:27]([CH:31]([CH3:33])[CH3:32])[C:26]=1[N:34]=[C:35]=[O:36])([CH3:24])[CH3:23]>>[CH:22]([C:25]1[CH:30]=[CH:29][CH:28]=[C:27]([CH:31]([CH3:32])[CH3:33])[C:26]=1[NH:34][C:35](=[O:36])[N:11]([CH2:10][C:7]1[CH:6]=[CH:5][C:4]([C:3]([N:2]([CH3:1])[CH3:21])=[O:20])=[CH:9][CH:8]=1)[C:12]1[CH:17]=[CH:16][C:15]([CH2:18][CH3:19])=[CH:14][CH:13]=1)([CH3:23])[CH3:24]

Participants

3

Reactant 2

HCID 922592,6-Diisopropylphenyl isocyanateHCID 21957966HCID 21957966, compound

Product 1

HCID 21957915HCID 21957915, compound

Procedure

By the reaction and treatment in the same manner as in Example 1 using N,N-dimethyl-4-[(4-ethylphenyl)aminomethyl]benzamide (0.6 g) and 2,6-diisopropylphenyl isocyanate (0.46 mL) as starting materials, 4-[3-(2,6-diisopropylphenyl)-1-(4-ethylphenyl)ureidomethyl]-N,N-dimethylbenzamide (0.34 g) was obtained. melting point: 170–172° C.

Sources & evidence

ORD record
ord-8efa295c1ad94779bcaf7ddbc3972abc
Source dataset
uspto-grants-2006_09
Patent number
US07105567B2

Reaction notes

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