HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl bromide → HCID 178450473, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl bromide | HCID 8002 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 857653-89-5 | HCID 57954392 | — |
| Catalyst | Tetrabutylammonium Iodide | HCID 67553 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178450473 | HCID 178450473 | — |
Reaction Steps
A solution of 4-(3-pyridin-4-yl-[1,2,4]oxadiazol-5-yl)cyclohexylmethanol (Preparation 6) in THF was treated with sodium hydride, 1-bromobutane and tetrabutylammonium iodide, as described for Example 104, to afford the title compound: RT=4.16 min, m/z (ES+)=316.3
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08207147B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-f4dec724d7fb4622abb894ddc88b9d58 |
| Source note | uspto-grants-2012_06 |