2,6-Diisopropylphenyl isocyanate → HCID 10298086, compound

HRID 2213644Notes

Reaction equation

HRID 2213644 reaction equation
[CH3:1][N:2]([CH3:19])[C:3]1[CH:8]=[CH:7][C:6]([CH2:9][NH:10][C:11]2[CH:16]=[CH:15][C:14]([CH3:17])=[CH:13][C:12]=2[CH3:18])=[CH:5][CH:4]=1.[CH:20]([C:23]1[CH:28]=[CH:27][CH:26]=[C:25]([CH:29]([CH3:31])[CH3:30])[C:24]=1[N:32]=[C:33]=[O:34])([CH3:22])[CH3:21]>>[CH:20]([C:23]1[CH:28]=[CH:27][CH:26]=[C:25]([CH:29]([CH3:30])[CH3:31])[C:24]=1[NH:32][C:33](=[O:34])[N:10]([CH2:9][C:6]1[CH:5]=[CH:4][C:3]([N:2]([CH3:19])[CH3:1])=[CH:8][CH:7]=1)[C:11]1[CH:16]=[CH:15][C:14]([CH3:17])=[CH:13][C:12]=1[CH3:18])([CH3:21])[CH3:22]

Participants

3

Reactant 2

HCID 922592,6-Diisopropylphenyl isocyanateHCID 3709822HCID 3709822, compound

Product 1

HCID 10298086HCID 10298086, compoundYield 43.4%

Procedure

By the reaction and treatment in the same manner as in Example 1 using [(4-dimethylaminophenyl)methyl](2,4-dimethylphenyl)amine (1.0 g) and 2,6-diisopropylphenyl isocyanate (1.2 g) as starting materials, N′-(2,6-diisopropylphenyl)-N-[(4-dimethylaminophenyl)methyl]-N-(2,4-dimethylphenyl)urea (0.78 g) was obtained. melting point: 100° C.

Sources & evidence

ORD record
ord-e3ff16ca96a44300b372d091f39d1e07
Source dataset
uspto-grants-2006_09
Patent number
US07105567B2

Reaction notes

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