2,6-Diisopropylphenyl isocyanate → HCID 21957918, compound

HRID 2213652Notes

Reaction equation

HRID 2213652 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[CH2:9][NH:10][C:11]1[CH:16]=[CH:15][C:14]([CH:17]([CH3:19])[CH3:18])=[CH:13][CH:12]=1.[CH:20]([C:23]1[CH:28]=[CH:27][CH:26]=[C:25]([CH:29]([CH3:31])[CH3:30])[C:24]=1[N:32]=[C:33]=[O:34])([CH3:22])[CH3:21]>>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[CH2:9][N:10]([C:11]1[CH:12]=[CH:13][C:14]([CH:17]([CH3:19])[CH3:18])=[CH:15][CH:16]=1)[C:33]([NH:32][C:24]1[C:23]([CH:20]([CH3:21])[CH3:22])=[CH:28][CH:27]=[CH:26][C:25]=1[CH:29]([CH3:31])[CH3:30])=[O:34]

Participants

3

Reactant 2

HCID 922592,6-Diisopropylphenyl isocyanateHCID 21957904HCID 21957904, compound

Product 1

HCID 21957918HCID 21957918, compoundYield 9.4%

Procedure

By the reaction and treatment in the same manner as in Example 2 using [(2,4-dichlorophenyl)methyl](4-isopropylphenyl)amine (2.7 g) and 2,6-diisopropylphenyl isocyanate (2.1 g) as starting materials, N-[(2,4-dichlorophenyl)methyl]-N′-(2,6-diisopropylphenyl)-N-(4-isopropylphenyl)urea (0.43 g) was obtained.

Sources & evidence

ORD record
ord-791cfcf5393744d9834633435836e5d1
Source dataset
uspto-grants-2006_09
Patent number
US07105567B2

Reaction notes

Loading…