HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lawesson's reagent → HCID 57954389, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lawesson's reagent | HCID 87949 | — |
| Reactant | 4-{2-Oxo-2-[N'-(pyridine-4-carbonyl)-hydrazino]-ethoxy}-piperidine-1-carboxylic acid tert-butyl ester | HCID 69077736 | — |
| Product | HCID 57954389 | HCID 57954389 | — |
Reaction Steps
4-{2-Oxo-2-[N′-(pyridine-4-carbonyl)hydrazino]ethoxy}piperidine-1-carboxylic acid tert-butyl ester (Preparation 16) was treated with Lawesson's reagent in a similar manner to that described in Example 138, affording the title compound: RT=3.47 min, m/z (ES+)=377.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08207147B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-77af700898644a54a22be986535c6b7f |
| Source note | uspto-grants-2012_06 |