HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzonitrile → 2-(Phenylethynyl)furan
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzonitrile | HCID 7505 | — |
| Reactant | 2-Furonitrile | HCID 69245 | — |
| Product | 2-(Phenylethynyl)furan | HCID 11019252 | 74% |
Reaction Steps
The procedure was identical to Example 1, with the exception that 2-furonitrile (0.175 ml; 0.186 g; 2.00 mmol) was used as a substrate instead of benzonitrile. GC analysis of the organic phase of the hydrolyzed reaction sample after 18 h at 65° C. showed the presence of 1.26 mmol (74% yield) of 2-(phenylethynyl)furan and no remaining 2-furonitrile in the reaction mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07105707B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-a4b01b0c6e964a4cacdaf67e42468670 |
| Source note | uspto-grants-2006_09 |