HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 86656263, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 3-(4-Bromo-benzenesulfonylamino)-benzoic acid | HCID 2302232 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86656263 | HCID 86656263 | — |
Reaction Conditions
| Temperature | 0 °C |
|---|
Reaction Steps
A suspension of 3-(4-bromophenylsulfonamido)benzoic acid (2.30 g, 6.46 mmol) in DCM (50 mL) was stirred and cooled under argon to 0° C. Oxalyl chloride (676 μL, 7.11 mmol) was then added dropwise via a syringe, followed by DMF (50 μL). The resulting solution was then stirred overnight, allowing the reaction mixture to warm room temperature. The solution was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08207167B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-983c01d1b1d44e2096d9a9d1c4cb9ec4 |
| Source note | uspto-grants-2012_06 |