HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3-Nitrophenyl)-1,2-ethanediol → 1-(3-Aminophenyl)ethane-1,2-diol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3-Nitrophenyl)-1,2-ethanediol | HCID 14997031 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1-(3-Aminophenyl)ethane-1,2-diol | HCID 14997033 | 119.6% |
Reaction Steps
1-(3-Nitrophenyl)ethane-1,2-diol (10 g) was dissolved in MeOH (100 ml). 10% Pd/C (1.3 g) was added the mixture hydrogenated at 40 psi H2 for 1 hour. The reaction mass was filtered through hyflo and concentrated to give the crude title compound (10 g, 92%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08207167B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-f3392fe8c9b445eb8034e7ed591a7a26 |
| Source note | uspto-grants-2012_06 |