3-Bromotoluene → HCID 57122906, compound

HRID 221413Notes

Reaction equation

Br[C:2]1[CH:3]=[C:4]([CH3:8])[CH:5]=[CH:6][CH:7]=1.[F:9][C:10]1[CH:15]=[C:14]([F:16])[CH:13]=[CH:12][C:11]=1B(O)O>>[F:9][C:10]1[CH:15]=[C:14]([F:16])[CH:13]=[CH:12][C:11]=1[C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH3:8])[CH:3]=1

Participants

Reactant 2

HCID 115603-Bromotoluene

HCID 27343342,4-Difluorophenylboronic acid

Product 1

HCID 57122906HCID 57122906, compound

Procedure

Using a method analogous to Method B, using 3-bromotoluene and 2,4-difluorobenzene boronic acid, the title compound was obtained as a clear oil.

Sources & evidence

ORD record: ord-a3c2c32b057d48a7a55350e50b363ce7
Source dataset: uspto-grants-2012_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08207167B2

Reaction notes

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