Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 6-Aminoquinoline | HCID 11373 | — |
| Reactant | 2-Chloronicotinic acid | HCID 76258 | — |
| Product | HCID 21959464 | HCID 21959464 | — |
Reaction Steps
A mixture of 2-chloronicotinic acid (1.5 g) and 6-aminoquinoline (1.4 g) was heated at 140° C. neat for 2 h. The reaction was cooled to give a brown solid used in the next step without further purification. MS (ES+): 266 (M+H)+; (ES−): 264 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07105682B2 |
|---|
| Source dataset | uspto-grants-2006_09 |
|---|
| ORD ID | ord-c550787156e44c87a98ab15c08bd3b99 |
|---|
| Source note | uspto-grants-2006_09 |
|---|
