HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethylaniline → HCID 7021723, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethylaniline | HCID 949 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Phenylpropionic acid, (+)- | HCID 2724622 | — |
| Solvent | Tetrachloroethylene | HCID 31373 | — |
| Product | HCID 7021723 | HCID 7021723 | 102.4% |
Reaction Steps
Into a 10 L four-necked flask, 600 g (4.00 mol) of (S)-2-phenylpropionic acid, 2.4 L of tetrachloroethylene, 951 g (8.00 mol) of thionyl chloride and a small amount of dimethyl aniline were added, followed by stirring at room temperature overnight, and excess of thionyl chloride and tetrachloroethylene were distilled off under reduced pressure to obtain 691 g of (S)-2-phenylpropionic chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07108895B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-6d9b29fc548a42f1a1e8bd38817b10e6 |
| Source note | uspto-grants-2006_09 |