HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 21948216, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | N-(3-chlorophenyl)-4-(2-chloropyridin-4-yl)pyrimidin-2-amine | HCID 9905031 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21948216 | HCID 21948216 | — |
Reaction Steps
A mixture of (3-chloro-phenyl)-[4-(2-chloro-pyridin-4-yl)-pyrimidin-2-yl]-amine (4.8 g, 0.015 mol) in hydrazine (20 ml, 0.41 mol) is refluxed for 90 minutes. The reaction is poured into ethanol (300 ml) with efficient stirring. The resulting precipitate is filtered with suction to yield the title compound, m.p. 201–203° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07109197B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-cfffb7989bbf41838f6a8f0fdaba6a50 |
| Source note | uspto-grants-2006_09 |