HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzaldehyde → HCID 74058495, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzaldehyde | HCID 68023 | — |
| Reactant | tert-Butyl bromoacetate | HCID 79177 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Product | HCID 74058495 | HCID 74058495 | 84% |
Reaction Steps
Condensation of 4-fluorobenzaldehyde with hydroxylamine hydrochloride using the same procedure as Compound 44-A followed by reaction with tert-butyl bromoacetate gave the title oxime ether as a clear oil (84% yield). 1HNMR 400 MHz (CDCl3) δ (ppm): 1.52 (9H, s, t-Bu), 4.61 (2H, s, OCH2), 7.08 (2H, m, aromatics), 7.59 (2H, m, aromatics), 8.19 (1H, s, CH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07109186B2 |
| Source dataset | uspto-grants-2006_09 |
| ORD ID | ord-ef0bd93ca8474c31999f47010e05f80a |
| Source note | uspto-grants-2006_09 |